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GCMS analysis results for sample AD28044, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD28044 conducted on January 2, 2002.

NYC-WTC_000034516–000034526

Folder label: “GCMS X 11/21/01 A 12/21/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28044.D Vial: 35 Acq On : 22 Dec 2001 1:12 am Operator: GALOS Sample : gems unknown 11/21 Inst :•GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.782 317 321 332 rVB 172378 342957 3.68% 0.693% 2 11.789 753 758 772 rVB 3367018 7047013 75.71% 14.238% 3 15.402 1145 1152 1169 rBV 3963364 9308180 100.00% 18.807% 4 20.675 1719 1727 1746 rBV 3693699 9005370 96.75% 18.195% 5 25.095 2200 2209 2219 rBV2 3708637 8437124 90.64% 17.047%

6 33.100 3074 3082 3096 rBV2 2677374 6651652 71.46% 13.439% 7 35.622 3351 3357 3371 rBV 1580229 3495407 37.55% 7.062% 8 37.172 3517 3526 3538 rBV2 1817416 5206351 55.93% 10.519%

Sum of corrected areas: 49494054

28044.D NP112701.M Thu Dec 27 08:38:03 2001

NYC-WTC_000034522

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NYC-WTC_000034522Source: NYC Law Department, mirrored locally

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