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GCMS analysis results for sample AD28048, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD28048 conducted on January 2, 2002.

NYC-WTC_000034537–000034547

Folder label: “GCMS X 11/21/01 A 12/21/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File : C:\HPCHEM\1\DATA\DEC2101\28048.D Vial: 33 Acq On : 21 Dec 2001 11:23 pm Operator: GALOS Sample : gems unknown 11/21 Inst :.GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.783 317 321 332 rVB 207119 417829 4.78% 0.905% 2 11.791 753 758 769 rVB 3186812 6676395 76.36% 14.466% 3 15.404 1145 1152 1163 rBV 3865134 8742791 100.00% 18.944% 4 20.686 1719 1728 1745 rBV 3651936 8468119 96.86% 18.348% 5 25.096 2200 2209 2218 rBV2 3472498 7984603 91.33% 17.301%

6 33.093 3074 3081 3093 rBV2 2649051 6525323 74.64% 14.139% 7 35.624 3350 3357 3373 rBV 988379 2264557 25.90% 4.907% 8 37.173 3517 3526 3539 rBV2 1813413 5071988 58.01% 10.990%

Sum of corrected areas: 46151605

28048.D NP112701.M Thu Dec 27 08:39:10 2001

NYC-WTC_000034543

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NYC-WTC_000034543Source: NYC Law Department, mirrored locally

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