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GCMS analysis results, sample AD28045, Jan 2 2002

Machine-extracted title · confidence 87%

Gas chromatography-mass spectrometry analysis of environmental sample AD28045 identifying unknown compounds and surrogate standard 2,4-DDD, completed January 2, 2002.

NYC-WTC_000034495–000034504

Folder label: “GCMS X 11/21/01 A 12/21/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

- Data File : C:\HPCHEM\1\DATA\DEC2101\28045.D Vial: 29 Acq On : 21 Dec 2001 8:38 pm Operator: GALOS Sample : gems unknown 11/21 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.988 10 16 22 rVB 52445 103115 1.20% 0.234% 2 7.712 309 313 317 rBV 59819 107182 1.25% 0.243% 3 7.776 317 320 334 rVB 418515 826686 9.61% 1.872% 4 11.793 753 758 768 rBV 3172042 6599607 76.74% 14.948% 5 15.406 1145 1152 1168 rBV 3645990 8599399 100.00% 19.477%

6 20.678 1719 1727 1750 rBV 3429569 8355151 97.16% 18.924% 7 25.098 2199 2209 2218 rBV2 3444842 7904444 91.92% 17.903% 8 33.095 3073 3081 3095 rBV2 2676094 6546991 76.13% 14.829% 9 37.175 3516 3526 3537 rBV2 1826444 5108197 59.40% 11.570%

Sum of corrected areas: 44150772

28045.D NP112701.M Thu Dec 27 08:38:19 2001

NYC-WTC_000034501

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NYC-WTC_000034501Source: NYC Law Department, mirrored locally

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