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GCMS analysis results for sample AD28105, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD28105 conducted on January 2, 2002.

NYC-WTC_000034642–000034652

Folder label: “GCMS X 11/23/01 A 12/21/01

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Scanned page image, NYC-WTC_000034648
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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File : C:\HPCHEM\l\DATA\DEC2101\28105.D Vial: 12 Acq On : 22 Dec 2001 3:56 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.963 6 13 17 rBV2 35653 71761 1.05% 0.205% 2 6.504 177 181 185 rBV 46234 93812 1.37% 0.268% 3 7.760 314 318 334 rBB 406578 860070 12.58% 2.456% 4 11.795 752 758 771 rVB 2611849 5327293 77.95% 15.211% 5 15.399 1145 1151 1169 rBV 3194963 6834552 100.00% 19.514%

6 20.681 1720 1727 1736 rBV 3033069 6614729 96.78% 18.887% 7 25.083 2200 2207 2217 rBV2 2837908 6296550 92.13% 17.978% 8 29.732 2710 2714 2720 IBB 72162 138252 2.02% 0.395% 9 33.088 3072 3080 3093 rBV2 2266118 5032501 73.63% 14.369% 10 37.160 3514 3524 3535 rBV2 1394014 3753688 54.92% 10.718%

Sum of corrected areas: 35023208

28105.D NP112701.M Fri Dec 28 09:55:01 2001

NYC-WTC_000034648

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NYC-WTC_000034648Source: NYC Law Department, mirrored locally

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