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GCMS analysis results, sample AD28324, Jan 2002

Machine-extracted title · confidence 95%

GCMS analysis results for sample AD28324 dated January 3, 2002, showing surrogate compound results.

NYC-WTC_000035550–000035560

Folder label: “GCMS X 11/28/01 A 12/28/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File : C:\HPCHEM\1\DATA\DEC2801\28324 .D Vial: 10 Acq On 28 Dec 2001 4:08 pm Operator: GALOS Sample : gems unknown 11/28 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.028 15 20 24 rBV 58659 102242 1.65% 0.328% 2 7.752 313 317 320 rBV 52275 90810 1.46% 0.292% 3 7.816 320 324 338 rVB 476429 913745 14.72% 2.935% 4 11.832 757 762 775 rVB 2350161 4692204 75.57% 15.070% 5 15.445 1149 1156 1170 rBV 2734821 6209090 100.00% 19.941%

6 20.718 1723 1731 1746 rBV 2740057 5896004 94.96% 18.936% 7 25.129 2204 2212 2222 rBV2 2607120 5539132 89.21% 17.790% 8 33.125 3077 3084 3096 rBV2 1887720 4336438 69.84% 13.927% 9 33.391 3109 3113 3128 rVB 70110 169509 2.73% 0.544% 10 37.206 3521 3529 3544 rBV2 1176855 3187615 51.34% 10.237%

Sum of corrected areas: 31136789

28324.D NP112701.M Mon Dec 31 10:09:53 2001

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NYC-WTC_000035556

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NYC-WTC_000035556Source: NYC Law Department, mirrored locally

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