GCMS analysis report, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC2101\28308.D Vial: 40 Acq On 22 Dec 2001 4:43 pm Operator: GALOS Sample gems unknown 11/26 Inst ■ : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Ether, 3-butenyl propyl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

10.23 0.51 ng/uL 137030 1,4-Dichlorobenzene-d4 11.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ether, 3-butenyl propyl 114 C7H140 034061-75-1 12 2 Oxirane, 2-pethyl-3-propyl-, cis- 100 C6H120 006124-90-9 9 3 Hexane, 2 -methyl - 100 C7H16 000591-76-4 9 4 Pentanal, 2-methyl- 100 C6H120 000123-15-9 9 Abundance Scan 587 (10.226 min): 28308.D (-) m/z 43.10 100.00% i I 43

5000 55 59 39 73 85 „ > • i _ J 1 • ’ i • ---44 i miz-> 20 I | I I I I | ITTTp- 4I • ’r ■ ............... 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 TTT 100 T' 11 1 I 111'1 1' 11 I 9.80 m/z 10.00 10.20 10.40 10.60 59.10 40.83% Abundance #3059: Ether, 3-butenyl propyl 43

5000 ■ ' i ' ■ \.................... I T I I I .... I i . 9.80 10.00 10.20 10.40 10.60 m/ z 40.11% 30 391 55 73 85 55'10 I . ........ I ill . ....... " i" " i T" 1' I i" " I l' |" l • । ■ • । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1531: Oxirane, 2-methyl-3-propyl- cis- 48 \ A 1 1 ‘ 4 57 9.80 10.00 10.20 10.40 10.60 5000 71 85 m/ Z 41.10 33.70%

I i1 ■ ! 1 100 1 • • i1 *'11' TTTTTTTT i111' i11" i 1‘" > | r > i i p r TTT > . i . । > i > . , I TTTTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63434: Hexane, 2-methyl- S ■ ■ i ■ ■ 43 9.80 10.00 10.20 10.40 10.60 m/z 57.1,0 30.55% 5000 57 85 29 39 miz-> ..... 1.1..... — ........ . ....... 69 Tr TIWWUTT 100 11.1111 > I I > I t I I I I f I I I I I t I I I I I -r. । r . , r p-

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 i • • ■ • i ■ • 9.80 10.00 10.20 10.4C 10.60 ■ • ' I ' '

28308.D NP112701.M Fri Dec 28 09:09:36 2001 Page 4

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