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Document / 15 pages

GCMS analysis report, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS results for sample AD28172 analyzed on January 3, 2002.

NYC-WTC_000035381–000035395

Folder label: “GCMS X 11/26/01 A 12/22/01”

←Page 12 of 15→
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28308.D Vial: 40 Acq On : 22 Dec 2001 4:43 pm Operator: GALOS Sample : gems unknown 11/26 Inst • : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.44 0.58 ng/uL 157569 1,4-Dichlorobenzene-d4 11.78

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 2-Hexanol. 102 C6H140 000626-93-7 38 2 2-Pentano 4-methyl- 102 C6H140 000108-11-2 37 3 2-Pentano 4 2-Pent/no 4-methyl- 102 C6H140 000108-11-2 32 4-methyl- 102 C6H140 000108-11-2 32 Abundance Scan 610 (10.437 min): 28308.D (-) m/ z 43.10 100.00% 48

5000

57 85 39 61 69 10.00 10.20 10.40 10.60 10.80 ! mmmm 4 16 ■ ■ । ■ 11 TTPNTTT ‘O‘"TITT m/z 45.10 72.41% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63583: 2-Hexanol 45

--A-- -11 5000 - 10.00 10.20 10.40 10.60 10.80 m/ z 41.10 31.83% 27 31 39 42 , 55 58 84 87 • i '' ■ ■ i'' '' i1 ■ •' i ■''' i'' ■' I' TIt Trr • i • ■ • ■ । • ■ •»। ’1 • ■ i • • • • i ■ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1773: 2-Pentanol, 4-methyl- 45 s 'I 1 1 1 1 1 ' 1 10.00 10.20 10.40 10.60 10.80 5000 m/z 85.15 21.56% I I 27 42 57 69| 84 87 ! 1 | TTTTTT . . . । . j , , ,, , TTTT । | । « । । । i I । । । i~i । i । । । t r T | 1 1 1 ' | 111 ' | • • « • | । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63547: 2-Pentanol, 4-methyl- A IT i 45 10.00 10.20 10.40 10.60 10.80 I m/ z 57.10 17.47% i 5000 -

27

m/z-> ... I.. —3s 4 20 25 30 35 40 45 ‘I[T 50 — ...”....... 55 60 65 69

70 11' " ' I' 75 80 84 87 11' । ■1 ■ ■ । ■11' i ■ ■

85 90 95 11." ... A ' ' I 1 ' ' ’ I ‘ ' 1 ' I • ‘ 10.00 10.20 10.40 10.60 10.80

28308.D NP112701.M Fri Dec 28 09:09:38 2001 Page 5

NYC-WTC_000035392

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NYC-WTC_000035392Source: NYC Law Department, mirrored locally

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