GCMS analysis comments for sample AD28689, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\28689.D Vial: 14 Acq On ‘5 Dec 2001 1:04 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 1-Octadecanol Concentration Rank 11

•R.T. EstConc Area Relative to ISTD R.T.

29.68 0.72 ug/1 141358 Chrysene-dl2 33.03

Hit# of 5/ Tentative ID MW MolForm CAS# Qual

1 1-Octadecanol 270 C18H380 000112-92-5 74 2 4-Tetyadecanol 214 C14H30O 001653-33-4 74 3 1-Eicosanol 298 C20H42O 000629-96-9 72 4 Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 70 Abundance Scan 2684 (29.684 min): 28689.D (-) m/z 42.95 100.00% 43

83 5000 55 69 97 111

-138 ............... 125 110 ... A 29.40 29.60 29.80 30.00

m/z—> —40 a60+ 80 100 120 140 160 180 200 224 ■ ■ i > ‘ 220 ‘ i ■ ■ ■ ■ i 240 m/ z 83.05 54.31% Abundance #72029:1-Octadecanol 43 55 69 83 97 5000 ' TPrr 111 29.40 29.60 29.80 30.00 125 m/ z 55.00 48.40% i ■ ' ■ 1 i 1 224 252 1 i 1 1 ' 1 1 1 1 1 ' I miz-> Abundance ■ ■ i ' ‘ 40 60 80 100 120 140 160 180— 200 ‘ 220 240 #26420; 4-Tetradecanol 43 57 83 97 — -A - 29.40 29.60 29.80 30.00 5000 m/z 56.95 45.58% 70 111 : I i 125 — | 166 196 T miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #72723:1-Eicosanol 43 55 _ 29-40 29.60 29.80 30.00 m/z 60.95 45.48% 83 97 5000 71 111 125 .................. — I 139 I ,i 252 ■ ' i 1 ' ITT 111 40 60 80 100 120. 140 160 180 200 220 240 29.40 29.60 29.80 30.00 _

28689.D GCMS1126.M Mon Dec 10 10:19:13 2001 Page 4

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