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GCMS analysis comments for sample AD28695, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting recovery data and acceptance range issues for sample AD28695.

NYC-WTC_000035106–000035114

Folder label: “GCMS X 11/24/01 A 12/4/01

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Scanned page image, NYC-WTC_000035110
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0401\28695.D Vial: 10 Acq On 4 Dec 2001 9:10 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 11.712 721 726 746 rBV 1599493 4191504 72.67% 14.715% 2 15.311 1113 1118 1134 rBV 2493172 5530968 95.89% 19.418% 3 20.589 1686 1693 1716 rBV 2581927 5767857 100.00% 20.250% 4 25.005 2168 2174 2187 rBV2 2373404 5207150 90.28% 18.281% 5 25.152 2187 2190 2201 rVB2 21430 64722 1.12% 0.227% 6 29.439 2652 2657 2665 rBV 114030 223391 3.87% 0.784% 7 30.082 2721 2727 2736 rBV 310703 644306 11.17% 2.262% 8 31.569 2885 2889 2895 rBV2 43230 99980 1.73% 0.351% 9 33.038 3042 3049 3065 rBV2 1570944 3741989 64.88% 13.137% 10 37.132 3487 3495 3516 rBV2 1034534 3012052 52.22% 10.575%

Sum of corrected areas: 28483919 28695.D GCMS1126.M Thu Dec 06 15:20:33 2001

NYC-WTC_000035110

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NYC-WTC_000035110Source: NYC Law Department, mirrored locally

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