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GCMS analysis comments for sample AD28690, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report noting bis(2-ethylhexyl)phthalate detection and recovery data for sample AD28690.

NYC-WTC_000035044–000035051

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C: \HPCHEM\ 1 \DATA\DEC 0401\28690.D Vial: 20 Acq On : 5 Dec 2001 6:55 am Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.663 281 285 293 rBV 27359 77764 1.34% 0.277% 2 11.712 721 726 746 rBV 1623283 4203215 72.37% 14.964% 3 15.311 1113 1118 1137 rBV 2518484 5527159 95.17% 19.677% 4 20.589 1686 1693 1719 rBV 2620400 5807634 100.00% 20.676% 5 25.005 2168 2174 2186 rBV2 2381789 5206693 89.65% 18.536% 6 25.152 2186 2190 2196 rVB2 21403 63496 1.09% 0.226% 7 29.439 2652 2657 2662 rBV2 52309 110620 1.90% 0.394% 8 30.082 2721 2727 2734 rBV 308378 648176 11.16% 2.308% 9 33.038 3042 3049 3062 rBV2 1554384 3637492 62.63% 12.950% 10 33.313 3073 3079 3088 rBV 37436 98019 1.69% 0.349% 11 37.132 3487 3495 3511 rBV2 940986 2709174 46.65% 9.645%

Sum of corrected areas: 28089442 28690.D GCMS1126.M Thu Dec 06 13:24:00 2001

NYC-WTC_000035048

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NYC-WTC_000035048Source: NYC Law Department, mirrored locally

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