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GCMS analysis results sample AD29459, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29459 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036447–000036457

Folder label: “GCMS X 12/5/01 A 12/12/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1201\29459.D Vial: 26 Acq On : 13 Dec 2001 3:21 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.593 274 278 308 rBV 302560 953278 13.44% 2.655% 2 11.348 683 687 692 rBV 76547 186416 2.63% 0.519% 3 11.421 692 695 711 rW 86965 263427 3.71% 0.734% 4 11.669 715 722 746 rBV 1978864 . 5241734 73.88% 14.597% 5 15.277 1109 1115 1133 rBV 2930092 6505506 91.69% 18.117%

6 20.556 1683 1690 1712 rBV 3114219 7095176 100.00% 19.759% 7 24.972 2165 2171 2184 rBV2 2953664 6482075 91.36% 18.052% 8 30.048 2718 2724 2735 rBV 423633 861115 12.14% 2.398% 9 33.004 3039 3046 3068 rBV2 2007575 4692728 66.14% 13.069% 10 37.099 3484 3492 3507 rBV2 1277362 3627167 51.12% 10.101%

Sum of corrected areas: 35908622

29459.D GCMS1126.M Fri Dec 21 12:26:09 2001

NYC-WTC_000036452

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NYC-WTC_000036452Source: NYC Law Department, mirrored locally

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