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Document / 11 pages

GCMS analysis comments for sample AD29022, Dec 17 2001

Machine-extracted title · confidence 95%

Lab notes for sample AD29022 indicate no unusual compounds detected but one LCS compound outside acceptance range.

NYC-WTC_000035820–000035830

Folder label: “GCMS X 11/30/01 A 12/10/01

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Scanned page image, NYC-WTC_000035825
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

'Data File : C:\HPCHEM\1\DATA\DEC1001\29022.D Vial: 9 Acq On : 10 Dec 2001 6:33 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.599 274 278 292 rBV 347277 928057 13.71% 2.699% 2 11.354 683 687 691 rBV 46357 110076 1.63% 0.320% 3 11.427 691 695 710 rVB 57577 174739 2.58% 0.508% 4 11.675 716 722 746 rBV 1835879 4839084 71.46% 14.074% 5 15.274 1108 1114 1132 rBV 2896565 6221079 91.87% 18.094%

6 20.553 1683 1689 1710 rBV 3082867 6771625 100.00% 19.695% 7 24.968 2164 2170 2183 rBV2 2731801 6281524 92.76% 18.269% 8 30.045 2718 2723 2730 rBV 428906 869127 12.83% 2.528% 9 33.010 3038 3046 3057 rBV2 1830116 4550291 67.20% 13.234% 10 37.096 3483 3491 3511 rBV2 1281877 3637198 53.71% 10.579%

Sum of corrected areas: 34382800

29022.D GCMS1126.M Wed Dec 12 16:03:03 2001

NYC-WTC_000035825

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NYC-WTC_000035825Source: NYC Law Department, mirrored locally

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