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GCMS sample analysis results, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30085 conducted on January 9, 2002.

NYC-WTC_000019061–000019069

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC2101\30085.D Vial: 7 Acq On : 22 Dec 2001 12:42 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.606 275 279 310 rBV 392613 1181796 16.88% 3.355% 2 11.360 685 688 693 rBV 28446 71100 1.02% 0.202% 3 11.443 693 697 703 rW2 27466 74611 1.07% 0.212% 4 11.673 717 722 746 rBV 1969491 5181061 74.02% 14.707% 5 15.280 1109 1115 1134 rBV 2755194 6469472 92.43% 18.364%

6 20.550 1683 1689 1712 rBV 2958594 6999224 100.00% 19.868% 7 24.975 2165 2171 2184 rBV2 2693852 6393462 91.35% 18.149% 8 30.052 2719 2724 2733 rBV 417358 880400 12.58% 2.499% 9 33.008 3040 3046 3067 rBV2 1725561 4575061 65.37% 12.987% 10 37.102 3484 3492 3513 rBV 1148864 3402120 48.61% 9.657%'

Sum of corrected areas: 35228307

30085.D GCMS1126.M Wed Jan 02 10:10:51 2002

NYC-WTC_000019066

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NYC-WTC_000019066Source: NYC Law Department, mirrored locally

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