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GCMS sample analysis results, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30313 conducted on January 9, 2002.

NYC-WTC_000019100–000019110

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\l\DATA\DEC2101\30313.D Vial: 14 Acq On : 22 Dec 2001 7:31 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.600 274 278 313 rBV 449304 1284368 17.42% 3.639% 2 11.354 683 687 692 rBV 54492 130623 1.77% 0.370% 3 11.437 692 696 704 rW 49698 141439 1.92% 0.401% 4 11.666 716 721 747 rBV 2140304 5695516 77.26% 16.135% 5 15.274 1109 1114 1132 rBV 3022810 6808485 92.36% 19.289%

6 20.553 1683 1689 1710 rBV 3310876 7371538 100.00% 20.884% 7 24.969 2164 2170 2184 rBV2 2597129 6456270 87.58% 18.291% 8 30.055 2718 2724 2736 rBV 345153 745254 10.11% 2.111% 9 33.011 3039 3046 3071 rBV 1549326 3952088 53.61% 11.196% 10 37.105 3484 3492 3504 rBV2 872104 2712537 36.80% 7.685%

Sum of corrected areas: 35298118

30313.D GCMS1126.M Wed Jan 02 10:16:53 2002

NYC-WTC_000019105

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NYC-WTC_000019105Source: NYC Law Department, mirrored locally

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