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GCMS sample analysis results, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30260 conducted on January 9, 2002.

NYC-WTC_000019081–000019089

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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Scanned page image, NYC-WTC_000019086
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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\1\DATA\DEC2101\30250.D Vial: 9 Acq On : 22 Dec 2001 2:39 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R. T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.593 274 278 312 rVB 376463 1112600 16.32% 3.258% 2 11.669 717 722 746 rBV 1957969 4944320 72.51% 14.479% 3 15.277 1109 1115 1133 rBV 2661483 6190619 90.79% 18.129% 4 20.556 1683 1690 1711 rBV 2946298 6818754 100.00% 19.969% 5 24.971 2165 2171 2186 rBV2 2525567 6261230 91.82% 18.336%

6 30.048 2718 2724 2737 rBV 369575 829271 12.16% 2.429% 7 33.013 3040 3047 3073 rBV 1817414 4642228 68.08% 13.595% 8 37.108 3485 3493 3519 rBV 1063922 3348181 49.10% 9.805%

Sum of corrected areas: 34147203

30250.D GCMS1126.M Wed Jan 02 10:14:13 2002

NYC-WTC_000019086

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NYC-WTC_000019086Source: NYC Law Department, mirrored locally

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