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GCMS analysis results, sample AD30022, January 2002

Machine-extracted title · confidence 75%

Gas chromatography-mass spectrometry analysis of sample AD30022 conducted January 9, 2002, measuring organic compounds with 80% surrogate recovery.

NYC-WTC_000016708–000016716

Folder label: “GCMS X 12/12/01 A 12/19/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\l\DATA\DEC1901\30022.D Vial: 8 Acq On : 20 Dec 2001 6:18 am Operator: 209 GALOS Sample : gc/ms scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.603 275 279 314 rBV 298327 987490 13.47% 2.704% 2 11.670 717 722 748 rBV 1877111 5210369 71.06% 14.269% 3 15.278 1109 1115 1134 rBV 2960720 6702926 91.42% 18.357% 4 20.556 1683 1690 1717 rBV 3251420 7331887 100.00% 20.079% 5 24.972 2165 2171 2185 rBV2 2807616 6616673 90.25% 18.121%

6 30.049 2719 2724 2735 rBV 373656 828702 11.30% 2.269% 7 33.014 3040 3047 3066 rBV2 2032925 5025392 68.54% 13.763% 8 37.109 3485 3493 3517 rBV 1260142 3811365 51.98% 10.438%

Sum of corrected areas: 36514804

30022.D GCMS1126.M Wed Jan 02 16:04:48 2002

NYC-WTC_000016713

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NYC-WTC_000016713Source: NYC Law Department, mirrored locally

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