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GCMS sample analysis results, Jan 2002

Machine-extracted title · confidence 50%

GCMS analysis of environmental sample AD30021 conducted January 9, 2002.

NYC-WTC_000016699–000016707

Folder label: “GCMS X 12/12/01 A 12/19/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\l\DATA\DEC1901\30021.D Vial: 7 Acq On : 19 Dec 2001 3:38 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.603 275 279 309 rBV 295880 944740 15.20% 2.965% 2 11.669 717 722 746 rBV 1644723 4514248 72.65% 14.167% 3 15.277 1110 1115 1134 rBV 2477218 5666842 91.19% 17.784% 4 20.556 1684 1690 1713 rBV 2798588 6214100 100.00% 19.501% 5 24.972 2165 2171 2185 rBV2 2371015 5751170 92.55% 18.048%

6 25.119 2185 2187 2205 rVB3 26560 110079 1.77% 0.345% 7 27.001 2385 2392 2402 rBV 51117 133022 2.14% 0.417% 8 30.058 2719 2725 2735 rVB 317773 660963 10.64% 2.074% 9 33.014 3040 3047 3068 rBV2 1842006 4529292 72.89% 14.214% 10 37.108 3485 3493 3521 rBV2 1105475 3341114 53.77% 10.485%'

Sum of corrected areas: 31865570

30021.D GCMS1126.M Wed Jan 02 16:04:11 2002

NYC-WTC_000016704

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NYC-WTC_000016704Source: NYC Law Department, mirrored locally

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