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GCMS analysis results for sample AD30087, Jan 2002

Machine-extracted title · confidence 50%

GCMS analysis of environmental sample AD30087 conducted January 9, 2002.

NYC-WTC_000016737–000016745

Folder label: “GCMS X 12/12/01 A 12/19/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\l\DATA\DEC1901\30087.D Vial: 14 Acq On : 20 Dec 2001 2:08 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF . Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.600 274 278 291 rBV 395176 968556 13.43% 2.644% 2 7.738 291 293 303 rVB3 24850 83075 1.15% 0.227% 3 11.438 693 696 711 rVB2 25281 94689 1.31% 0.258% 4 11.667 717 721 740 rBV 1973523 5187965 71.92% 14.160% 5 15.275 1109 1114 1133 rBV 2967786 6610846 91.65% 18.044%

6 20.554 1683 1689 1714 rBV 3284712 7213338 100.00% 19.688% 7 24.979 2164 2171 2185 rBV2 2832469 6682974 92.65% 18.241% 8 30.056 2719 2724 2738 rBV 378513 788313 10.93% 2.152% 9 33.012 3040 3046 3069 rBV2 2029233 5193471 72.00% 14.175% 10 37.106 3482 3492 3515 rBV2 1270036 3814779 52.89% 10.412%

Sum of corrected areas: 36638006

30087.D GCMS1126.M Wed Jan 02 16:06:03 2002

NYC-WTC_000016742

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NYC-WTC_000016742Source: NYC Law Department, mirrored locally

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