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GCMS sample analysis results, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30314 conducted on January 9, 2002.

NYC-WTC_000019121–000019129

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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Scanned page image, NYC-WTC_000019126
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NYC 9/11 Public Portal Document LSC Area Percent Report

•Data File : C:\HPCHEM\l\DATA\DEC2101\30314.D Vial: 5 Acq On : 22 Dec 2001 10:45 am Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF . Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.609 275 279 311 rBV 457375 1286267 16.55% 3.390% 2 11.364 684 688 693 rBV 28683 80893 1.04% 0.213% 3 11.437 693 696 704 rW 29375 85338 1.10% 0.225% 4 11.676 716 722 746 rBV 2216988 5839929 75.12% 15.392% 5 15.274 1109 1114 1134 rBV 3139763 7235798 93.08% 19.072%

6 20.553 1683 1689 1718 rBV 3517590 7774088 100.00% 20.490% 7 24.978 2164 2171 2184 rBV2 2886750 6941820 89.29% 18.297% 8 30.055 2718 2724 2734 rBV 424650 876867 11.28% 2.311% 9 33.011 3039 3046 3064 rBV2 1834728 4515976 58.09% 11.903% 10 37.105 3482 3492 3522 rBV2 1087751 3303135 42.49% 8.706%'

Sum of corrected areas: 37940111

30314.D GCMS1126.M Wed Jan 02 10:17:42 2002

NYC-WTC_000019126

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NYC-WTC_000019126Source: NYC Law Department, mirrored locally

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