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GCMS analysis results, sample AD30315, Jan 2002

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Gas chromatography-mass spectrometry analysis report for sample AD30315, completed January 9, 2002, showing unknown compounds data.

NYC-WTC_000019163–000019173

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC2101\30315.D Vial: 6 Acq On : 22 Dec 2001 11:44 am Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF. Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.611 276 280 310 rBV 287177 941446 15.51% 3.089% 2 11.366 685 689 693 rBV 29238 74232 1.22% 0.244% 3 11.439 693 697 704 rW 28727 81151 1.34% 0.266% 4 11.669 717 722 749 rBV 1547660 4595829 75.73% 15.079% 5 15.277 1109 1115 1133 rBV 2409887 5592329 92.15% 18.348%

6 20.556 1683 1690 1715 rBV 2634441 6068396 100.00% 19.910% 7 24.971 2165 2171 2215 rBV2 2178962 5787573 95.37% 18.989% 8 30.057 2719 2725 2736 rBV 292994 634361 10.45% 2.081% 9 33.013 3040 3047 3065 rBV2 1566501 3956836 65.20% 12.982%, 10 37.108 3484 3493 3513 rBV 877619 2746788 45.26% 9.012%

Sum of corrected areas: 30478941

30315.D GCMS1126.M Wed Jan 02 10:18:48 2002

NYC-WTC_000019168

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NYC-WTC_000019168Source: NYC Law Department, mirrored locally

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