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Document / 8 pages

GCMS analysis comments for sample AD28680, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS scan results for sample AD28680, noting phthalate detection and recovery rates.

NYC-WTC_000035000–000035007

Folder label: “GCMS X 11/24/01 A 12/4/01

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Scanned page image, NYC-WTC_000035004
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C : \HPCHEM\ 1 \DATA\DEC04 0128669.D Vial: 9 Acq On : 4'Dec 2001 8:11 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.777 293 298 313 rBV 49816 188322 3.56% 0.717% 2 11.707 721 726 750 rBV 1348376 3854082 72.78% 14.676% 3 15.314 1113 1119 1137 rBV 2394449 5050658 95.37% 19.232% 4 20.584 1687 1693 1710 rBV 2399963 5295594 100.00% 20.164% 5 25.009 2168 2175 2187 rBV2 2163079 4771119 90.10% 18.167%

6 25.156 2187 2191 2203 rVB2 19648 63009 1.19% 0.240% 7 30.076 2722 2727 2733 rBV 289327 584739 11.04% 2.227% 8 33.032 3043 3049 3065 rBV2 1519967 3543959 66.92% 13.495% 9 33.317 3074 3080 3091 rVB 29644 81149 1.53% 0.309% 10 37.127 3488 3495 3520 rBV2 984339 2829335 53.43% 10.774%

Sum of corrected areas: 26261966 28669.D GCMS1126.M Thu Dec 06 13:20:53 2001

NYC-WTC_000035004

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NYC-WTC_000035004Source: NYC Law Department, mirrored locally

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