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GCMS analysis results for sample AD27818, Jan 2002

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Laboratory report documenting GCMS analysis of environmental sample AD27818 conducted on January 3, 2002.

NYC-WTC_000033641–000033652

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27818.D Vial: 29 Acq On : 19 Dec 2001 6:34 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.290 132 136 144 rBV 78999 170004 2.00% 0.402% 2 6.391 144 147 158 rW2 95002 294297 3.47% 0.697% 3 6.529 158 162 171 rW 50826 137702 1.62% 0.326% 4 6.639 171 174 189 rVB 53033 155507 1.83% 0.368% 5 11.660 716 721 757 rBV 2312488 6074603 71.53% 14.378%

6 15.277 1109 1115 1134 rBV 3322735 7870601 92.68% 18.628% 7 20.556 1683 1690 1714 rBV 3806349 8492255 100.00% 20.100% 8 24.981 2165 2172 2184 rBV2 3427723 8090497 95.27% 19.149% 9 33.014 3040 3047 3069 rBV2 2481641 6210020 73.13% 14.698% 10 37.108 3485 3493 3518 rBV 1661108 4755151 55.99% 11.255%

Sum of corrected areas: 42250637

27818.D GCMS1126.M Wed Jan 02 12:05:52 2002

NYC-WTC_000033646

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NYC-WTC_000033646Source: NYC Law Department, mirrored locally

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