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GCMS analysis results for sample AD27772, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AD27772 conducted on January 3, 2002.

NYC-WTC_000033593–000033604

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27772.D Vial: 28 Acq On : 19 Dec 2001 5:36 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst :“GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.291 133 136 143 rBV 97972 212364 2.35% 0.467% 2 6.401 144 148 152 rW 132299 321038 3.56% 0.707% 3 6.530 159 162 171 rW 65392 166444 1.85% 0.366% 4 6.640 171 174 187 rVB 69745 188281 2.09% 0.414% 5 7.595 273 278 285 rBV 45745 118411 1.31% 0.261%

6 11.662 716 721 753 rBV 2468916 6509444 72.17% 14.329% 7 15.270 1109 1114 1133 rBV 3480352 8326853 92.32% 18.329% 8 20.557 1683 1690 1713 rBV 4018689 9019470 100.00% 19.854% 9 24.973 2165 2171 2185 rBV2 3601577 8584898 95.18% 18.897%' 10 25.120 2185 2187 2201 rVB2 33998 116853 1.30% 0.257% 11 33.015 3040 3047 3072 rBV2 2770479 6726845 74.58% 14.807% 12 37.110 3485 3493 3516 rBV2 1782784 5138846 56.98% 11.312%

Sum of corrected areas: 45429747

27772.D GCMS1126.M Wed Jan 02 12:02:04 2002

NYC-WTC_000033598

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NYC-WTC_000033598Source: NYC Law Department, mirrored locally

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