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GCMS analysis results for sample AD27771, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AD27771 conducted on January 3, 2002.

NYC-WTC_000033580–000033592

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27771.D Vial: 30 Acq On : 19 Dec 2001 7:33 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst :*GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.296 132 136 141 rBV 75259 162916 2.19% 0.438% 2 6.397 144 147 158 rW 105921 314562 4.22% 0.846% 3 6.525 158 161 170 rW 49383 134339 1.80% 0.361% 4 6.645 170 174 187 rVB 56590 150980 2.03% 0.406% 5 11.666 716 721 750 rBV 1986675 5313501 71.34% 14.293%

6 15.274 1108 1114 1134 rBV 2965803 6872933 92.28% 18.488% 7 20.553 1683 1689 1709 rBV 3409556 7447758 100.00% 20.034% 8 24.978 2164 2171 2184 rBV2 2964671 6944359 93.24% 18.680% 9 33.010 3040 3046 3067 rBV2 2276214 5516387 74.07% 14.839%' 10 37.105 3484 3492 3511 rBV2 1467485 4317353 57.97% 11.614%

Sum of corrected areas: 37175088

27771.D GCMS1126.M Wed Jan 02 12:00:38 2002

NYC-WTC_000033585

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NYC-WTC_000033585Source: NYC Law Department, mirrored locally

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