GCMS analysis results for sample AD27823, Jan 2002

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LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27823.D Vial: 31 Acq On : 19 Dec 2001 8:32 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst :.GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 6.290 132 136 143 rBV 58495 128884 2.21% 0.449% 2 6.391 144 147 153 rBV 70707 185631 3.18% 0.646% 3 6.529 158 162 171 rW 38047 108186 1.86% 0.377% 4 6.639 171 174 191 rVB2 39178 120958 2.07% 0.421% 5 11.661 716 721 747 rBV 1586385 4253283 72.94% 14.804%

6 15.269 1109 1114 1133 rBV 2217153 5410366 92.78% 18.832% 7 20.547 1683 1689 1710 rBV 2530251 5831232 100.00% 20.297% 8 24.972 2165 2171 2185 rBV2 2297734 5392100 92.47% 18.768% 9 33.014 3040 3047 3070 rBV2 1680883 4176082 71.62% 14.536%, 10 37.109 3485 3493 3517 rBV2 1016677 3123115 53.56% 10.871%

Sum of corrected areas: 28729837

27823.D GCMS1126.M Wed Jan 02 12:07:47 2002

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