NYC-WTC_000035776
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS calibration results for sample AD28662, Dec 2001
Machine-extracted title · confidence 100%Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
NYC-WTC_000034958–000034970Folder label: “GCMS X 11/24/01 A 12/4/01”
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NYC 9/11 Public Portal Document Library Search Compound Report • >Data File C:\HPCHEM\1\DATA\DECO4O1\LB.D Vial: 3 Acq On 4 Dec 2001 2:19 pm Operator: 209 GALOS Sample lb 11/24 Inst : GC/MS 209 Mise : Multiple: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C : \DATABASE\NBS75K . L ********************************************************************* Peak Number 5 Benzoic acid, 2,6-bis[(trimeth Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.81 1.13 ug/1 345108 Phenanthrene-dl0 25.00 Hit# of 5 Tentative ID MW MolForm CAS?! Qual
1 Benzoic acid, 2,6-bis [ (trimethylsil 370 C16H30O4Si3 003732-85-2 32 2 Phenethylamine, N-methyI-.beta., 3,4 399 C18H37NO3S13 010538-85-9 25 3 Noradrenaline, tetra- MS 457 C20H43NO3Si4 0000*0-00-0 25 4 N-(Trifluoroacetyl) ,0,0' ,O' ' -tetr 553 C22H42F3NO4 Si4 00000-00-0 22 Abundance Scan 1935 (22.810 min): LB.D (-) m/2 73.00 10 0.00% I 73
5000 355 ) 147 221 281 i 45 327 401 22.40 22.60 22.22 . 00 23.20 117 191 251 0- ■ ■11A ■,-,. — H+ I M -H - H+ - m/z 355.05 33.66% m/z->__ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360380 400 420 440 Abundance #51296: Benzoic acid, 2,6-bis[trimetnylsily!)oxy]-, triret 73 355
5000 1 | 22'40 22.60 22.80 23.00 23.20 147 267 m/z 147.00 1 29.75% : 47 j 208 237 । | PPTTTTTTP -----t-TTTRTmTTTTTT mz-> 40 60 80 100120140160180 200220240260280 300320340 360380400420440 Abundance #74239: Phenethylamine, N-methyl-.beia.,3,4-tris(trimethyls । 73 p . । t < . .. -t . ... | ■ 22.40 22.60 22.50 23.00 23.20 5000- 355 m/z 221.05 21.84% 44
mlz-> 1 147 193 267 294 — ‘T‘uI—"WIOTIETT‘TETTETT‘TET‘CCTECITTETT‘T‘‘T"TT j-rrn-p-nrTUTTTTTTT 40 60 80 100120140160180 200 220 240 260280 300320 340 350380 400 420440 Abundance #57357: Noradrenaline, tetra-TMS ——. .. .. rr — — , 111 73 22.40 22.60 22.80 23.00 23.20 m/z 281.00 17.51% i
5000 | 102 355
45 147 442 —1d0n/0do/n// ii EBLnTmT m/z—> 40 60 80 100120140160180200220240 260 280 300320 340 350380 400 420440 22.40 22.60 22.-3 13.00 23.20
LB.D GCMS1126.M Thu Dec 06 14:41:01 2001 Page 5
NYC-WTC_000034968
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