GCMS comments for sample AD28666, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2901\28649.D Vial: 48 Acq On : 30 Nov 2001 9:38 am Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Benzene-1,2,3,4-d4-, 5,6-dichl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.52 ug/1 117026 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Benzene- <2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 =? 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 3 Benzenamine, N-methyl-4-nitro- 152 C7H8N2021 000100-15-2 9 4 Acenaphthylene__________________ 152 C12H8 000208-96-8 9 Abundance Scan 710 (11.560 min): 28649.D (-) m/z 149.90 100.00% 150

5000 115 78 52 11.20 11.40 11.60 11.80 --- 40 I 62 87100 ............. A— m/z 151.90 58.63% m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 5000 52 78 11.20 11.40 11.60 11.80 m/z 114.90 . 35.52% 35 87 mPTPT 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

1l'2O 11.40 11.60 11.80........ 5000 115 m/z 78.05 21.21% 52 78

35 ' ’ I • ’ •' I • " • I '' I'' ■ ■ I' ' 87........ u......... I4—— I ■ ■ ’ ■ l ■ ■ ■' I " ■ ■ I ■'1' l' • • ■ I ■''' I'. mz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10120: Benzenamine, N-methyl-4-nitro- 1T*TTT "Ir 152 11.20 11.40 11.60 11.80 m/z52.0014.50% 77 122 110 5000 65 30 94 —.......... 46,............. .. ............. TII TITT 11 ■ ■ ■ ■ । • '~i • ■ ■ ■ n ■ ■ ■ i ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

28649.D GCMS1126.M Fri NOV 30 16:19:59 2001 Page 2

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