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GCMS comments for sample AD28600, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28600 analyzed in early December 2001.

NYC-WTC_000034741–000034749

Folder label: “GCMS X 11/23/01 A 11/29/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV2901\28475 .D Vial: 38 Acq On 29 NOV 2001 11:22 pm Operator: 209 GALOS Sample 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.53 ug/1 123961 1,4-Dichlorobenzene-d4 11.69 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorob .zene-d4 150 C6C12D4 003855-82-1 53 2 Benzenebutanoic acid, 3-nitro-.gamm 223 C10H9NO5i 006328-00-3 12 3 Benzene-1 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 10 4 Benzofura , 7-chloro-________________ 152 C8H5C10 024410-55-7 9 Abundance C Scan 710 (11.565 min): 28475.D (-) m/z 149.90 100.00% 150

5000 115 78 52 1120 11.40 11.60 11.80 38 , 66 J 89 npmnpmmmn m... I..... H'l।।।। 11 * 11111111111111 m/z 151.90 j 66.33% mz—> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 11.20 1l'4O 11.60 11.80 ' 52 m/z 114.90 38.53%

mz-> 35 87 " i •• ••!’" 'I " 11"" i" I ‘' I T A... — bl..1.... Ill .............. 30 40 50 60 70 80 90 100110120130140150160170180190200210220 I.... Id........................... ... f.. 11111II111111111111

Abundance #28308: Benzenebutanoic acid, 3-nitro-.gamma.-oxo- 150 11.20 11.40 11.60 11.80 5000 m/z 78.05 23.62% 56 104 76 | 159 mp .4 TTTT ........................ 92 122 134 206 223 TI’T ""I11 ,.... ।.... ।....,.. i. ।«k. ।. 11 mz-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 11.20 11.40 11.60 11.80 " 1 ' m/z 52.00 16.11% 115 5000 52 78

35 87 I | h_________ " i" " I" " i" " i ‘' r'" i" " i'1" i" " I"1' r " ■ i" " 11111111111"111111111111111111111U " " 1111111 ‘I T T m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 11.20 11.40 11.60 11.80

28475.D GCMS1126.M Fri Nov 30 14:40:43 2001 Page 2

NYC-WTC_000034748

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NYC-WTC_000034748Source: NYC Law Department, mirrored locally

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