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GCMS comments for sample AD28594, Dec 2001

Machine-extracted title · confidence 100%

Laboratory analyst notes on GCMS scan results detecting bis(2-ethylhexyl)phthalate and recovery rates for sample AD28594.

NYC-WTC_000034750–000034758

Folder label: “GCMS X 11/23/01 A 11/29/01

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Scanned page image, NYC-WTC_000034757
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2 901\28600.D Vial: 39 Acq On : 30 Nov 2001 12:20 am Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.52 ug/1 120551 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichloro] nzene-d4 003855-82-1 64150 C6C12D4 2 Benzene-l, 2,3,4-d4-, 5,6-dichloro- 002199-69-1 23150 C6C12D4 3 Benzofur. , 7-chloro- 024410-55-7 9 152 C8H5C10 4 1H-Pyrro o[2,3-b]pyridine-2,6-dione 152 C7H8N2021 ____ 017384-56-4 9 Abundance * Scan 710 (11.560 min): 28600.D (-) Tm/z 149.90 100.00% 150

5000 115 52 78 1120 11.40 11.60 11.80

mz-> 38 63 .. ......... T A I" " I 207 .. 111TIWUTT.4 30 40 50 60 70 80 90 100 110120130140150160 170180 190 200 210 m/z 151.90 65.13% Abundance #9593: 1,4-Dichlorobenzene-d4 1$0

5000 115 78 11.20 11.40 11.60 11.80 52 m/z 115.00 . 35.06% 87 mlz-> 35 JU .I....I.H q .HIH H | I bI | H ri | b... |.... ..r.1.... p i|u.... r...f 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 | ,

Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0 TT TT TT 115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 20.24%

35 87 I mmmmm I' |' > H H ' j " • ■ lmmm " l" • • I' ‘" I ■" i" " i ■' m/z-> 30 40 50 60 70 80 90 100110120130140 150160170180190 200 210 Abundance #10136: Benzofuran, 7-chloro- —————————— , T TTrTr 1$2 11-20 11.40 11.60 11.80 m/z 52.00 17.75% 5000 89

63 35 49 , 73 125 TTTI"TT‘T THTT TTTTIT’T’TT I" " I m/z—> 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 1l'20 11.40 11.60 11.80

28600.D GCMS1126.M Fri Nov 30 14:49:58 2001 Page 2

NYC-WTC_000034757

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NYC-WTC_000034757Source: NYC Law Department, mirrored locally

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