GCMS blank analysis report for sample AD28593, Nov-Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\LBC.D Vial: 4 Acq On : 27 Nov 2001 8:13 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.52 ug/1 101158 1,4-Dichlorobenzene-d4 11.69 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2, 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 33 3 4-Amino-2- chlorobenzonitrile 152 C7H5C1N2 020925-27-3 10 4 Benzonitrile, 2-amino-5-chloro- 152 C7H5C1N2 ____ 005922-60-1 10 Abundance Scan 710 (11.565 min): LBC.D (-) m/z 149.90 .100.00% 150

5000 115 78 T T 1 1 -ni 1 1 1 52 111 ■ , 3844, i . . .61........... ................ I................ . T I i-j-r-r ‘LL’ET ' I 1 ' ' 1 I ' ' 1 ' TT’TIII’IITTT ——— 1120 11.40 11.60 11.80 m/z 151.90 . 63.03% mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 110

5000 115 52 78 11.20 11.40 11.60 11.80 ' m/z 115.00 . 37.84% 35 ■ ■ । • ■ ■ • । > 87 i '' ’ ' i ' ’ .1,1.............. L 100 110 120' 130 140 150 ....... 160 m/z-> 30 40 50 60 70 80 90 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 ■ i ■ ' ' ■ i ' ' ‘ T ■ ' ' ' I ' ' ' ' i ■ 115 11 20 11.40 11.60 11.80 5000 52 78 m/z 77.95 . 19.37%

miz-> Abundance 35 ....... I 30 40 50 ■ i ■ ■ ■ ■ i' 60 70 87 1 11 ■ ■ ■ ■ । ■ 80 90 #10110:4-Amino-2-chlorobenzonitrile T + । ■ ■ ■ ■ 1 100 110 120 130 140 150 160 41 ■ i • ■ ’ ■ 1 ■ ■ ■ ■ l ■ ■ ■ ■ r1■ ■ ■ । ' 11 2 11.20 11.40 11.60 11.80 m/z 52.00 . 13.18% 5000

m/z—> 63 ■' i' ■ ■' i ■ ■ ■ ■ i ■ • ■' 11 ■ ■ ’ i ■ 30 40 50 60 70 76 11 f I" 80 90

90 ..... 117125 100 110 120 ....... 130 140 150 160 1 ■ ■ i ■ ■ 11.20 1140 11.60 11.80 '

LBC.D GCMS1126.M Fri NOV 30 16:06:55 2001 Page 3

NYC-WTC_000034739