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GCMS comments for sample AD28149, Nov 2001

Machine-extracted title · confidence 100%

Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

NYC-WTC_000033765–000033779

Folder label: “GCMS X 11/20/01 A 11/26/01”

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28159.D vial: 21 Acq On : 27 NOV 2001 6:15 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise t Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.51 ug/1 125960 1,4-Dichlorobenzene-d4 11.69 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-/,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 1,2,5-Trithiepane 152 C4H8S3 006576-93-8 10 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 10 Abundance Scan 709 (11.556 min): 28159.D (-) m/z 149.90 100.00% 150

5000 115 78 —1T——n—TTTLTETTTT 52 11.20 11.40 11.60 11.80

m/z-> 30 TCT 4444 —++2 44 — 38 40 T .T T103 . TTTTTTr 1— m/z 151.90 . 65.64% TTTTTT 70 80 90 100 110 120 130 140 150 160 50 60 Abundance ' 1, ’ . 150

5000 115 T TTTTn—r 78 11.20 11.40 11.60 11.80 52 m/z 115.00 37.06% 35 87 - '11' <' • । > I' T‘ TT T-rpr-TT-rp-T miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 11.20 11.40 11.60 11.80 5000 52 78 1 77.95 17.28%

35 87 TTIITTPTTT TII-ICIIII [, ---P L ।, । — 1— m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10068:1,2,5-Trithiepane TTTTTTTTTPTUTPTTTT 152 11.20 11.40 11.60 11.80_____ m/z 52.00 15.30%

5000 60 87 45 124

' TT TTTT TTfr i T ' i 78 TTTTTTTT , T 96 16 i'1111 1' I' — ————— m/z—> 30 40 50 60 70 80 90 100 11 120 130 140 150 160 11.20 11.40 11.60 11.80

28159.D GCMS1126.M Wed NOV 28 11:15:48 2001 Page 1

NYC-WTC_000033772

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