GCMS comments for sample AD28153, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data Pile : C:\HPCHEM\1\DATA\NOV2601\28143 .D Vial: 14 Acq On : 26 NOV 2001 11:25 pm Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.56 0.50 ug/1 122383 1,4-Dichlorobenzene-d4 11.69

Hit# of/ 5 Tentative ID MW MolForm CAS# Qual

1 1,4/Dichlorobenzene-d4 150 C6C12D4 003855-82-1 50 2 B enzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 enzaldehyde, 2-hydroxy-3 -methoxy- 152 C8H803 000148-53-8 10 4 B iphenylene 152 C12H8 000259-79-0 9 Abundance Scan 710 (11.565 min): 28143.D (-) m/z 149.90 100.00% 150

5000 115 52 78 11.20 11.40 11.60 11.80 —. HH 1A.38 | 63 । 80 90 — 111" " i1 ■ 100 110 120 130 140 150 160 m/z 151.90 62.40% mlz-> 30 40 50 60 70 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 ' 1 1 11 ''1 ' 1 TTT1 । 'T 1 1 ' I ' 78 1120 11.40 11.60 11.80 52 m/z 114.90 , 34.19% 87 mz-> 30 35 ■ ■ i ■ ■'' i' ''' I 40 50 ' ' I' • ■ ' I ■ • 60 70 80 '' I ■''' i ■ 90 —L 100 110 120 130 140 150 160 T l Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

5000 52 78 115 m/z I ' i ■ ' ■ ■ l ' ' ' ' I ' ■ ' ' I 1 ' ' ’ P 1120 11.40 11.60 11.80

miz-> Abundance 35 ... 1.... 30 40 50 ■ ' i1 ' ' ' I ' ' 60 70 80 87 1 i ’ ’ ■ ■ i ■''' i ■ ■ ■ ■ i ’' 90 100 110 120 130 #66892: Benzaldehyde, 2-hydroxy-3-methoxy- + 1-— 140 150 160

152 11.20 11.40 11.60 11.80 m/z 52.00 13.91% 106 5000 53 81

122

m/z—> 1 ■ i1 ■' ■ i ■ ■ ■ ■ i 30 40 50 - 60 70 TP 92 80 90 100 —. 1 136 ■ i'' ' ' i ' ■ ■ ' i 110 120 130 140 150 160 11.20 11.40 11.60 11.80

28143.D GCMS1126.M Tue Nov 27 15:29:59 2001 Page 1

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