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GCMS analysis results for sample AD27678, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27678 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033247–000033262

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data .File C:\HPCHEM\l\DATA\DEC1901\27678.D Vial: 5 Acq On 19 Dec 2001 10:48 am Operator: GALOS Sample gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of ■ # min scan scan scan TY height area % max. total

1 5.133 29 32 35 rBV 34654 61413 1.00% 0.189% 2 5.188 35 38 53 rVB 54233 123610 2.02% 0.381% 3 6.554 184 187 197 rW2 50055 124593 2.04% 0.384% 4 6.802 209 214 224 rBV 36545 84046 1.37% 0.259% 5 7.747 313 317 321 rBV 99201 182988 2.99% 0.564%

6 7.820 321 325 332 rW 620374 1219798 19.92% 3.758% 7 10.277 588 593 600 rBV 182426 333860 5.45% 1.029% 8 10.488 611 616 623 rBV 234750 423577 6.92% 1.305% 9 10.809 647 651 658 rVB 144676 265436 4.34% 0.818% 10 11.846 759 764 775 rVB 2456459 4826022 78.83% 14.869%

11 15.459 1151 1158 1174 rBV 2999689 6122404 100.00% 18.863% 12 20.731 1726 1733 1743 rBV 2724677 5794245 94.64% 17.852% 13 25.133 2205 2213 2224 rBV2 2442838 5358635 87.53% 16.510% 14 33.139 3079 3086 3102 rBV2 1870635 4159155 67.93% 12.815% 15 37.219 3523 3531 3545 rBV2 1229943 3376719 55.15% 10.404%

Sum of corrected areas: 32456501

27678 .D NP112701.M Thu Dec 20 11:41:00 2001

NYC-WTC_000033253

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NYC-WTC_000033253Source: NYC Law Department, mirrored locally

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