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GCMS analysis results for sample AD27276, Jan 2002

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Laboratory report documenting GCMS analysis of environmental sample AD27276 conducted on January 3, 2002.

NYC-WTC_000033043–000033066

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

■ Data File : C:\HPCHEM\1\DATA\DEC1901\27276.D Vial: 4 Acq On. 19 Dec 2001 8:56 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Smoothing OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs 0.2 Max Peaks: 100 Stop Thrs 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.151 30 34 38 rW 37901 67921 1.10% 0.216% 2 5.206 38 40 48 rVB 48529 95674 1.55% 0.305% 3 6.462 174 177 184 rBB 35705 66768 1.09% 0.213% 4 6.572 184 189 199 rBV2 61132 145752 2.37% 0.464% 5 6.701 199 2 03 210 rBV3 30174 68133 1.11% 0.217%

6 6.811 210 215 221 rBV 39630 81741 1.33% 0.260% 7 7.755 314 318 322 rBV 165310 296113 4.81% 0.944% 8 7.829 322 326 337 rVB 412495 857367 13.93% 2.732% 9 10.277 588 593 602 rBB 219943 379027 6.16% 1.208% 10 10.488 611 616 623 rBV 281685 487720 7.93% 1.554%

11 10.809 647 651 658 rBV 180757 324225 5.27% 1.033% 12 11.845 759 764 775 rBV 2474116 4824278 78.40% 15.373% 13 15.458 1151 1158 1175 rBV 2925661 6153034 100.00% 19.607% 14 20.731 1725 1733 1745 rBV 2676132 5709232 92.79% 18.193% 15 25.133 2206 2213 2225 rBV2 2322008 5066328 82.34% 16.144%

16 33.138 3079 3086 3099 rBV2 1695048 3708789 60.28% 11.818% 17 37.210 3523 3530 3546 rBV2 1115292 3049931 49.57% 9.719%

Sum of corrected areas: 31382033

27276.D NP112701.M Wed Dec 19 09:57:37 2001

NYC-WTC_000033049

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NYC-WTC_000033049Source: NYC Law Department, mirrored locally

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