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GCMS results log, sample AD27056, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27056 completed on December 10, 2001.

NYC-WTC_000032627–000032637

Folder label: “GCMS X 11/9/01 A 12/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File 2 \H PCH I ! \ 1 \ D. TA \ DEC 0 5 01 \ 2 7 0 5 5 . D Vial: 10 Acq On Dec 2001 5:11 pm Operator: GALOS Sample : :,Is unknown 11/13 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integrate Harams: LSCINT.P

Quant Metho:': . C:\KPCTEM\1\METHODS\NP112701.M (RTE Integrator) Title . 118 525/TCLP calibration table Library : C:\DATABASR\NBS75K.L ************* • Peak Number 2 Concentration Rank 1

R.T. EstC ■ : rea Relative to ISTD R.T. 25.16 20.0 - 1la 70 13 00 Phenanthrene-diO 25.31

Hit# of 5 tatit ID MW MolForm CAS# Qual

1 An t hr ac a n e 188 C14D10 001719-06-8 95 2 Phenant h r & • : ... 0 188 C14D10 001517-22-2 52 3 Antipyrine 188 C11H12N2O 000060-80-0 36 4 4-Methyl-2 EC .. i :.1)pyrimidi 188 C11H9FN2 076128-67-1 33 Abundance 1 1): 27055.D (-) m/z 188.10 100.00% 188 ft 5000 -

I0 160 24.80 25.00 25.20 25.40 25.60 42 52 :021121578 —132.14 HTTTTTT 170 180 PTm :* I1'"I m/z80.05 18.25% m/z—> 30 40 5. 00 _ 9 10112 120 130 140 150 160 170 180 190 Abundance • 19’ 5r A • ■ cene-d10- 188

5000 - TI । TT 24.80 25.00 25.20 25.40 25.60 m/z 94.05 16.59% 30 3-1 160 - TITTT i' ■ ■11 n/z-> 30 40 50 ' 0 1.0 1 " 0 130 140 150 160 170 180 190 Abundance ..' K 22: PI . . .;i:rene-d10 188 Tf — I" 24.80 25.00 25.20 25.40 25.60 5000- m/Z 187.20 15.35%

160 — m/z-> 30 40 50 co i • ■ ■ ■ i l..... 1_1 20 130 140 150 160 170 180 190 Abundance . 217.: ■ pyrine • I ' ' ' • I • ' ' ' p ’ l i I > I . . I I 188 24.80 25.00 25.20 25.40 25.60 m/z 189.10 14.63%

5000 U

■ । ■ ■ ■■ । • 129 ‘ *1' i11111 159 ( 173 1 '' I •''' r * “ i n ■ l ■ ■ ■ ' I • • --------- m/z-> 30 40 •.'■0 ‘1) 2) 130 140 150 160 170 180 190 24.80 25.00 25.20 25.40 25.60

27055.D Nil Dec 07 11:56:32 2001 Page 2

NYC-WTC_000032636

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NYC-WTC_000032636Source: NYC Law Department, mirrored locally

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