GCMS results log, sample AD26993, Dec 11 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26993.D Vial: 27 Acq On 7 Dec 2001 10:44 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclohexane, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.05 0.50 ng/uL 199141 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 4 lH-Pyrazole, 3-ethyl-4,5-dihydro- 98 C5H10N2 _________ 005920-29-6 58 'Abundance ’ Scan 23 (5.050 min): 26993.D (-) m/z 83.05 100.00% 1 55 83

5000 41 98

69

m/z-> tM + 1...65ul...... I v 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 T TTTTT 4 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z .55.10 93.66% Abundance #63236: Cyclohexane, methyl- i 55 83

5000 98 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 70 m/z ,41.05 49.00% 1 661

(A — +rrroTrr I ■ ।1'" ।' • i" ’' i ■ TT‘ TTTTTT TT" TIT miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- 55 83 A 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000- 98 m/z 98.05 48.74% 42 27 69

’TTTTTTTTTT TT ' i ■ ■" i "'' r " ' r ''' i''" I'''' i' ■' ■ i ■ ■'' i " ■ ■ i' " ' i ■ " ' I' ‘' i ■1'11 T’’ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 480 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- r’" ' i1 ■ ■■I■■■ ■ i ■ i ■ ■ 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z 42.10 32.36% 5000 98 42 69 27 -rpm-rp-m-p- I TP TTTTTTTTT Imppe TTTTTTTTT \AA 44 111' ‘ I TTT m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26993.D NP112701.M Tue Dec 11 14:55:44 2001 Page 1

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