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GCMS analysis results for sample AD26831, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26831 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032232–000032244

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0501\26831.D Vial: 6 Acq On 5 Dec 2001 1:19 pm Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclohexane, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.05 0.60 ng/uL 223349 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 96 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 96 4 1H-Pyrazole, 4,5-dihydro-4,5-dimeth 98 C5H10N2 _______ 028019-94-5 64 Abundance Scan 23 (5.054 min): 26831 .D (-) m/z 83.05 100.00%| 55 83

5000 41 98 69 l ’11 ’ I r 1••।‘‘ •i•••*i TIt 4.90 5.00 5.10 5.20 5.30 5.40 5.50

m/z-> 20 25 30 TH 35 40 I

45 51 11 +6— 111" 111 - TIH HTTTT 50 55 60 65 70 75 80 85 90 95 100 105 m/z 55.10 98.65% Abundance #63236: Cyclohexane, methyl- 55 83

5000 98 TTTIfT I ' 'I 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 70 m/ Z 46.26% I 661 m/z-> 20 11'11' i1 25 11' 30 I‘ TTT +rr frer ' ■ i'''' r 11 ■ ■ ■. । ■ 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Imprr Abundance #1326: Cyclohexane, methyl- 83 55 I'''' I'''' I 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.05 43.89% 42 27 69

'I' ‘1111" 11'•'' i ■ ■" i ■■" i'" ■ i •’■■i ■ I | I . I I | I TTTTTTTTTTT . | I . I I | . I ! I | I . I I | i""r' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- TIT i ■' ■ • i TUT 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50

N m/z 42.10 32.88% 5000 98 42 69 27 — m/z-> ' i " " r 1 " i' 20 25 30 111111 35 40 45 i11'1111 50 55 ---H 60 ' r " ■ r ' ■ ■ i'' 11" " i " 65 70 75 80 85 90 95 100 105 IETO001111—ETtrrTI i' ■ ■ ■ i 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26831.D NP112701.M Fri Dec 07 13:15:44 2001 Page 1

NYC-WTC_000032240

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