GCMS results log, sample AD26833, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26833.D Vial: 33 Acq On 7 Dec 2001 4:14 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclohexane, methyl- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

5.04 0.4 8 ng/uL/ 179649 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, 'methyl - 98 C7H14 000108-87-2 94 2 Cyclohexane/ methyl- 98 C7H14 000108-87-2 91 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 90 4 2-Pentene, 3,4-dimethyl- , (Z) - 98 C7H14 004914-91-4 64 Abundance Scan 21 (5.036 min): 2S833.D (-) m/z 83.05 100.00% 55 83

41 98 5000 70 I’F I > ' ■ ■ l ■ ■ ■ ■ l 4.90 5.00 5.10 5.20 5.30 5.40 5.50 II miz-> I " 111 ■' " I ll 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 77 11"11TT —mmmp .11 ■. । ।, m/ z 55.10 98.40% Abundance #1326: Cyclohexane, methyl- 55 83

- 5000- 98 27 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 69 m/z .41.10 51.01%

miz-> 'I " " 11 20 25 -rp- -m •i"'■i■ ITT i ■ ■" i 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- I 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 | 5000 98 m/z 98.15 45.76% 42 27 70

, 66 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i■ ■ ■' r '' ■ i''"r ''' r ' ■ ■ i'' ■' r ■ " r ■ ■1 r ■ ■■ i1 ■ ■ ■ i■ ■' ■ i1 ■'' r ■ " r " 11' " 1111 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- I’tt IIE-TTTETTT n 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z 42.10 34.30% 5000 98

LA.. 42 69 27 I 111 ’' 11111 mPPT +TT * I'"' I ’ • TTTTrIrr — MA A ' i " " r '' ‘I" l r" ' I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26833.D NP112701.M Tue Dec 11 14:46:30 2001 Page 1

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