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GCMS results log, sample AD26991, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26991 completed on December 11, 2001.

NYC-WTC_000032462–000032480

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data■File C:\HPCHEM\l\DATA\DEC0601\26991.D Vial: 17 Acq On 7 Dec 2001 12:43 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.032 15 21 26 rBV 89639 168172 2.07% 0.382% 2 6.472 174 178 186 rBV 36416 85105 1.05% 0.193% 3 6.582 186 190 193 rBV 51454 89775 1.11% 0.204% 4 7.847 324 328 343 rVB 606133 1287409 15.88% 2.922% 5 11.891 763 769 787 rBV 3172499 6497666 80.16% 14.747%

6 15.504 1157 1163 1180 rBV 3858779 8105741 100.00% 18.397% 7 20.777 1732 1738 1755 rBV 3856752 8003250 98.74% 18.164% 8 25.188 2212 2219 2231 rBV2 3449650 7519091 92.76% 17.065% 9 29.589 2694 2699 2707 rBV 125635 262827 3.24% 0.597% 10 29.699 2707 2711 2717 rVB 41058 86088 1.06% 0.195%

11 30.772 2823 2828 2838 rVB 51820 120174 1.48% 0.273% 12 31.717 2926 2931 2936 rBV 67674 170499 2.10% 0.387% 13 31.809 2936 2941 2953 rVB 114915 295236 3.64% 0.670% 14 32.799 3043 3049 3060 rBV 81093 241724 2.98% 0.549% 15 33.184 3085 3091 3109 rBV2 2517399 5774343 71.24% 13.105%

16 33.753 3147 3153 3166 rBV 77696 252486 3.11% 0.573% 17 34.661 3247 3252 3264 rBV2 42604 154643 1.91% 0.351% 18 35.550 3342 3349 3361 rBV 30226 114035 1.41% 0.259% 19 37.274 3529 3537 3555 rBV2 1716914 4832745 59.62% 10.968%

Sum of corrected areas: 44061009

26991.D NP112701.M Tue Dec 11 14:54:13 2001

NYC-WTC_000032468

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NYC-WTC_000032468Source: NYC Law Department, mirrored locally

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