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GCMS analysis report for sample AD26392, Dec 2001

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DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26392 noting other unknown compounds.

NYC-WTC_000031530–000031549

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV3001\26392.D Vial: 5 Acq On ? 30 Nov 2001 3:52 pm Operator: GALOS Sample ? gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr? 1.00 MS Integration Params? LSCINT.P

Method ? C?\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title ? 208 625/TCLP calibration table Smoothing ? OFF Filtering? 5 Sampling ? 1 Min Area? 1 % of largest Peak Start Thrs ? 0.2 Max Peaks? 100 Stop Thrs ? 0 Peak Location? TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation? 5

Signal ? TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.013 10 19 27 rBV2 128166 496196 4.37% 0.735% 2 5.114 27 30 34 rW 275843 524609 4.62% 0.777% 3 5.178 34 37 57 rVB 428348 1148358 10.12% 1.701% 4 5.664 87 90 106 rVB 71111 194132 1.71% 0.287% 5 6.122 136 140 155 rBV 237749 661263 5.83% 0.979% 6 6.471 173 178 182 rBV 75822 153207 1.35% 0.227% 7 6.572 186 189 200 rVB 76985 179659 1.58% 0.266% 8 6.709 200 204 206 rBV 75876 147270 1.30% 0.218% 9 7.186 249 256 278 rVB 1847617 4028245 35.49% 5.966% 10 7.846 324 328 342 rBV 1277334 2562320 22.58% 3.795% 11 9.359 489 493 504 rBV 51522 114697 1.01% 0.170% 12 10.322 593 598 608 rBV 489300 999036 8.80% 1.480% 13 10.533 617 621 631 rVB 230306 449428 3.96% 0.666% 14 11.744 748 753 762 rBV2 113337 245527 2.16% 0.364% 15 11.890 763 769 780 rW 4319979 8749882 77.10% 12.958% 16 15.503 1157 1163 1180 rBV 5604185 11348883 100.00% 16.807% 17 20.776 1731 1738 1750 rBV 5251825 10901839 96.06% 16.145% 18 25.187 2212 2219 2231 rBV2 4717616 10145763 89.40% 15.025% 19 33.192 3085 3092 3104 rBV2 3593213 7954454 70.09% 11.780% 20 37.282 3529 3538 3547 rBV 2420889 6519984 57.45% 9.656%

Sum of corrected areas? 67524752 26392.D NP112701.M Tue Dec 04 10:43:06 2001

NYC-WTC_000031536

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NYC-WTC_000031536Source: NYC Law Department, mirrored locally

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