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GCMS analysis results for sample AD26319, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26319 with unidentified compounds detected.

NYC-WTC_000031297–000031318

Folder label: “GCMS X 11/3/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C: \HPCHEM\1\DATA\DEC0501\26319 .D Vial: 7 Acq On 5 Dec 2001 2:13 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs ; 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.981 10 15 24 rBV2 78194 164351 2.17% 0.344% 2 5.101 26 28 32 rW 49044 8 0 8 04 1.07% 0.169% 3 5.165 32 35 46 rVB 67593 156251 2.06% 0.327% 4 6.100 133 137 143 rBV 41716 88479 1.17% 0.185% 5 6.449 170 175 183 rBV 39986 86851 1.15% 0.182%

6 6.559 183 187 197 rBV 45112 97243 1.28% 0.203% 7 7.824 321 325 342 rBV 1236047 2569227 33.93% 5.373% 8 10.300 591 595 607 rBV 43155 88906 1.17% 0.186% 9 11.868 761 766 776 rBV 2947067 6153718 81.26% 12.870% 10 12.703 348 857 861 rBV 32090 76671 1.01% 0.160%

11 14.500 1048 1053 1059 rVB 449205 822946 10.87% 1.721% 12 15.481 1154 1160 1178 rBV 3691329 7573101 100.00% 15.838% 13 17.645 1389 1396 1405 rBV 1095559 2129464 28.12% 4.453% 14 18.342 1467 1472 1477 rBV 71690 125688 1.79% 0.284% 15 20.460 1698 1703 1709 rBV 815939 1550598 20.61% 3.264%

16 20.754 1729 1735 1750 rBV 3598826 7406220 97.80% 15.489% 17 21.194 1777 1783 1788 rBV 139373 293145 3.87% 0.613% 18 22.973 1971 1977 1982 rBV 474783 963920 12.73% 2.016% 19 25.165 2207 2216 2227 rBV2 3041174 7228936 95.46% 15.118% 20 27.054 2416 2422 2429 rBV 216620 420613 5.55% 0.880%

21 28.814 2609 2614 2620 rVB 174683 339844 4.49% 0.711% 22 3 0 ;4 01 2782 2737 2792 rBV 140573 283443 3.74% 0.593% 23 31.859 2940 2946 2957 rBV 115042 262415 3.47% 0.549% 24 33.170 3082 3089 3110 rBV2 2099852 48*2797 64.34% 10.191% 25 34.509 3228 3235 3251 rBV 64255 1.99475 2.63% 0.417%

26 35.701 3360 3365 3376 rBV 33858 121617 1.61% 0.254% 27 37.251 3527 3534 3546 rBV2 1359955 3633955 48.05% 7.610%

Sum of corrected area:: 47815678

26319.D NP112701.M Wed Dec 05 15:07:27 2001

NYC-WTC_000031302

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NYC-WTC_000031302Source: NYC Law Department, mirrored locally

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