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GCMS results log, sample AD26985, Dec 11 2001

Machine-extracted title · confidence 95%

Laboratory report for GCMS analysis of sample AD26985 completed on December 11, 2001, showing surrogate recovery.

NYC-WTC_000032400–000032426

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.040 15 22 28 rBV 99508 187151 1.88% 0.326% 2 5.150 31 34 37 rBV 136644 233506 2.34% 0.407% 3 5.205 37 40 46 rVB 179637 326044 3.27% 0.568% 4 6.14 0 137 142 155 rVB 117863 275637 2.77% 0.480% 5 6.480 175 179 185 rBV 60890 121327 1.22% 0.211%

6 6.590 187 191 196 rBV 65491 134736 1.35% 0.235% 7 6.837 213 218 231 rVB2 40662 107786 1.08% 0.188% 8 7.177 248 255 265 rBV 168083 401367 4.03% 0.699% 9 7.855 325 329 346 rVB 612470 1372994 13.78% 2.392% 10 10.322 593 598 605 rBV 153295 308880 3.10% 0.538%

11 10.524 616 620 630 rBV 86496 177546 1.78% 0.309% 12 11.890 763 769 783 rBV 3854708 7923264 79.52% 13.804% 13 15.494 1156 1162 1180 rBV 4507712 9963435 100.00% 17.358% 14 20.776 1731 1738 1758 rBV 4682454 9856339 98.93% 17.171% 15 25.187 2212 2219 2230 rBV2 4291213 9260362 . 92.94% 16.133%

16 29.588 2694 2699 2707 rBV 359805 743670 7.46% 1.296% 17 29.698 2707 2711 2720 rVB 76121 167775 1.68% 0.292% 18 30.771 2823 2828 2840 rVB 87830 200954 2.02% 0.350% 19 31.716 2926 2931 2936 rBV 182831 456975 4.59% 0.796% 20 31.808 2936 2941 2953 rVB 205115 525178 5.27% 0.915%

21 32.798 3043 3049 3063 rBV 143968 420367 4.22% 0.732% 22 33.192 3085 3092 3113 rBV2 3096080 7231267 72.58% 12.598% 23 33.752 3147 3153 3169 rBV 137190 463128 4.65% 0.807% 24 34.659 3247 3252 3269 rBV 71220 265793 2.67% 0.463% 25 35.549 3344 3349 3363 rBV2 45252 188930 1.90% 0.329%

26 37.282 3529 3538 3557 rBV 2164285 6085788 61.08% 10.602%

NYC-WTC_000032406

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NYC-WTC_000032406Source: NYC Law Department, mirrored locally

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