GCMS method 208 data table, Dec 2001

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Library Search Compound Report Data File : C: \HPCHEM\1 \DATA\NOV3 001 \LB. D Vial: 2 Acq On : 30 Nov 2001 1:08 pm Operator: GALOS Sample : 1b 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.06 0.59 ng/uL 283512 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohe;xane, methyl- 98 C7H14 000108-87-2 96 3 Cyclohe:xane, methyl- 98 C7H14 000108-87-2 93 4 Cyclohexane, methyl - 98 C7H14 000108-87-2 78 Abundance Scan 23 (5.056 min): LB.D (-) m/z 83.05 100.00% 83 55

— n 11111 5000 41 98

70 4.90 5.00 5.10 5.20 5.30 5.40 5.50 36 , , 51,, , 63 79 i 91 m/z ‘I TTpauf 11[11111111111111 —p H — 55.05 78.95% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 83

5000 98 I ’ • ‘ * I T TMMg 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 70 m/z .98.15 49.00%

mz-> i “ ‘1 1 I ‘1 “ J * “ ’ I I“*‘i +- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 —pp ■f-p-rrrp-rn Abundance #63235: Cyclohexane, methyl- 55 83 ......../........................................ —! i . i . । i......।.i(■i i i । ■ 11 r j ■ 11 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 41.00 43.80% 42 69 27

m/z—> TIm—ug -rrp-m-p-r trrpr mHmmm — 1I——uun 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance . #1326: Cyclohexane, methyl- T’-T———1101117TTO—-"’1SSI1’T 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 55 m/z 56.10 26.34% 5000 98 42 27 69

TTpTTTyTTTT Hpu MHm — Iammagat mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

LB.D NP112701.M Tue Dec 04 10:13:48 2001 Page 1

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