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GCMS analysis results for sample AD26205, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report identifying ethoxy-benzoic acid and bis(2-Ethylhexyl)decanedioic acid in sample AD26205.

NYC-WTC_000031159–000031170

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV3001\26206.D Vial: 56 Acq On : 30 Nov 2001 8:34 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 d-Arabinose, cyclic 1,2-ethane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 7.01 0.56 ug/1 126010 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l d-Arab inose, cycli c/1,2-ethanediyl 394 C15H2208S2 040733-16-2 56 2 2-Propanone, 1-methoxy- 88 C4H802 005878-19-3 9 3 2-Butanol, 3-meh 1- 88 C5H120 000598-75-4 9 4 Butanoic acid, 3 ~hydroxy- 104 C4H803 000300-85-6 9 Abundance 7 Scan 215 (7.015 min): 26206.D (-) m/z 42.95 100.00% 4?

5000 73 i ■ • ' • i 1 • ■ ■ i ■ ■ ■ ■ i 1 ■ ' • i ’ ■ 6.60 6.80 7.00 7.20 7.40 - 88 207 m/z 44.95 95.03% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 S' 280 300 320 ' ‘ ‘' Abundance #53382: d-Arabinose, cyclic 1,2-ethanediyl mercaptal, tetra 45 105

5000 na—TTTTTTTTrr 61 6.60 6.80 7.00 7.20 7.40 m/z 73.0.0 28.58% 147 4 I . 85 I H t I 172189 274i 334 “ i ■11 ‘ i TITTT 11| 11 “ I ‘ i" I “ 111 '1 • l1 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #62920: 2-Propanone, 1-methoxy- 45 A/ i • ■ ■ 1 i ‘ 1 ■ • i । . 6.60 6.80 7.00 7.20 7.40 5000 m/z 61.00 28.44% 29

1411..... 88 i TT j m । fnnyn n I TH] ——————— . . । j .... j r। j ।. m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #62961:2-Butanol, 3-methyl- —1——uuuTTTTATTT 45 6.60 6.80 7.00 7.20 7.40 m/z 43.95 27.41% 5000

73 27 _ ___ ft ‘ * I TI 488 T-rp-n-q . > ।, ।.. >. j....।...11....।>...।...,|....।>.।. । ■... ।.... 11 - 1111 > 11... ] i,,, ।. i.. ।.. m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 26C280 300320 6.60 6.80 7.00 7.20 7.40

26206.D NP112601.M Mon Dec 03 09:42:01 2001 Page 1

NYC-WTC_000031167

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NYC-WTC_000031167Source: NYC Law Department, mirrored locally

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