GCMS analysis results for sample AD26164, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD26164 performed on December 3, 2001, noting other unknown compounds.

NYC-WTC_000031063–000031075

Folder label: “GCMS X 11/2/01 A 12/1/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26164.D Vials 61 Acq On : 1 Dec 2001 1:27 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 d-Arabinose, cyclic 1,2-ethane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 7.02 0.73 ug/1 164165 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 d-Arabinose, cyclic 1,2-ethanediyl 394 C15H2208S2 040733-16-2 43 2 2-Butanol, 3-methyl- 88 C5H120 000598-75-4 9 3 2-Butanol, 3-methyl-, (S) - 88 C5H120 001517-66-4 9 4 Propane/ 2-ethoxy-__________________ 88 C5H120 000625-54-7 9 Abundance Scan 216 (7.024 min): 26164. D(-) m/z 42.95 100.00% 43

5000 61 6.60 6.80 7.00 7.20 17.40 '___ | 1 1 1’88 i ■ ■ " i n . 111 207 11111’011’111020111 j .. i i j . i i , । : i I I | J I I i ] l i J J j . , 11—00111 m/z 44.95 95.04% vfz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #53382: d-Arabinose, cyclic 1,2-ethanediyl mercaptal, tetra 45 105

5000 ■ 1 i ' 1 1 ' i 1 ' 61 6.60 6.80 7.00 7.20 7.40 m/z 43.95 31.92% 147 ............................................................................................. 189 ......... 7334 —— 1 172 , ■ t... I, ■ 274 1’11 miz-> 20 40 60 80 100 120 1 40 160 180 200 220 240 260 280 300 320 Abundance #62961: 2-Butanol, 3-methyl- 45 111111 . . . . ( . , , , । . , , . । TT 6.60 6.80 7.00 7.20 7.40 5000 m/z 60.95 29.16%

73 27 ।, — — — miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #852:2-Butanol, 3-methyl-, (S)- 45 6.60 6.80 m/z 73.00 29.07%

5000

miz—> 27 73 । 1 .1 87 it, 1, T-IIt[TOI6192——19——9B9899[$9OIOOOID9—I933—C_99BI1TTCIIUS—O-""ITCC-STSTStI’S8411 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 A 6.60 6.80 ■i • ■ IPf 7.00 7.20 PTer 7.40

26164.D NP112601.M Mon Dec 03 12:20:12 2001 Page 1

NYC-WTC_000031071

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GCMS analysis report, Sample AD26164, Dec 2001 · Box DEP Box 21

NYC-WTC_000031076

Laboratory report documenting GCMS analysis of sample AD26164 for unknown compounds conducted on December 3, 2001.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999