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GCMS analysis results for sample AD26128, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26128 conducted on December 3, 2001.

NYC-WTC_000030980–000030991

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26128.D Vial: 65 Acq On 1 Dec 2001 5:21 am Operator: 209 GALOS Sample 11/2 gc/ms Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 d-Arabinose, cyclic 1,2-ethane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

7.06 0.97 ug/1 196173 1,4-Dichlorobenzene-d4 11.70

Hit# Of 5 Tentative ID MW MolForm CAS# Qual l d-Arabinose, cyclic 1,2-ethanediyl 394 C15H2208S2 040733-16-2 43 2 2-Propanone, 1-methoxy- 88 C4H802 005878-19-3 9 3 1-Propene, 1- (methylthio) - (E) - 88 C4H8S 042848-06-6 9 4 Ethanol, 2-chloro-, acetate_______ 122 C4H7C1O2 000542-58-5 9 Abundance 7 Scan 219 (7.056 min): 26128.D (-) m/z 42.95 100.00% 43

5000 73 TIpnmTgTTYifrr 88 6.80 7.00 7.20 7.40 ■ ■ ■ ■ i' — 158, 1 — 207 | I I I I | I 1 I I | I >'I I J I I I 1 | . . . . | . . . . | . . . . | . . ■ > ( • • • • | . • • t ( i ■ । . | ■ > ■ ■ | 4 m/z; 44.95 95.84% mz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #53382: d-Arabinose, cyclic 1,2-ethanediyl mercaptal, tetra 45 105

5000- " TT TT t । TI < । i । i j i 61 6.80 7.00 7.20 7.40 m/z 43*95 30.65% 1 ■ ■ i ■1111 T 1851 147 172 189 TTIIT .7TT 274 334 mz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #62920: 2-Propanone, 1-methoxy- 45 ' ' ‘ ' I ‘ ‘ I ' ' 1 ' I ' ' ‘ ' I ' ‘ ' 6.80 7.00 7.20 7.40 5000 m/z 73.0.0 29.72% 29

14.1L i ."i । i n » [ n i 88 •' ‘11 ‘1 ’11' ■ ■ ■ i ■ ■' ■ i “ ■' i1 ■ " i1 •' ■ i " " i " " i ■ ‘ " i'' “ i " ' ‘ i'" ■ i' miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #822:1-Propene, 1-(methylthio)-, (E)- TTT —1 T111— 45 73 88 6.80 7.00 7.20 7.40 m/z 60.95 28.83%

5000

- js_____________________________________________________________ ■ ■ i ■ ■ ■ ■ i' ‘I r" i1'" i" “ i ■ ■ ■ • i ■"' i ■ ■ ■■ I ■" ■ i ■ ■ ■' i" " i ■ ■■ ■ i •1 ■ ■ i ■ ■" i1 ■■ ■ i ■ ' rI 1 1 TT —Tmer ■ I " m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 6.80 7.00 7.20 7.40

26128.D NP112601.M Mon Dec 03 12:15:54 2001 Page 1

NYC-WTC_000030988

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