GCMS scan comments, Sample AD26133, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26133.D Vial: 59 Acq On : 30 Nov 2001 11:29 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 d-Arabinose, cyclic 1,2-ethane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

7.06 1.08 ug/1 264374 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 d-Arabinose, cyclic 1,2-ethanediyl 394 C15H2208S2 040733-16-2 40 2 2-Butanol, 3-methyl-, (S) - 88 C5H120 001517-66-4 9 3 2-Propanone, 1-methoxy- 88 C4H802 005878-19-3 9 4 1,2-Propanediol, 3-methoxy-106 C4H10O3 000623-39-2 9 Abundance Scan 219 (7.057 min): 26133.D (-) m/z 42.95 100.00% 43

5000

'' I ““ IH11 58 '" 73

88 [1 Tpuo , I । i i ,, TUTOIgg 207 T | 11 111 ! 111| i .— J.. m/z 6.80 7.00 44.95 7.20 7.40 98.51% ■nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #53382: d*Arabinose, cyclic 1,2-ethanediyl mercaptal, tetra 45 105

5000 61 6.80 7.00 ‘ ‘ 7.20 *17.40 • m/z 43.95 33.44% 147

miz-> ’ ’111 20 40 4s.| ........ 60 172189 e I1 . 274 334 11" ■ l' “' I' “ ‘ I “ “ I ‘ " I ‘' 1 • ■ • • l ‘ 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #852: 2-Butanol, 3-methyI-, (S)- 45

6.80 7.00 7.20 7.401 5000 m/z; 73.00 32.88%

73 —27 60 808 '" 11 ” 'l l I ...... ...... 100 120 140 160 180 200 220 240 260 280 300 *320 ‘ miz-> 20 40 Abundance #62920: 2-Propanone, 1-methoxy- TTPT 11* TTr 1 n 1 - 45 6.80 7.00 7.20 7.40 m/z 60.95 31.71%

5000 29

1411 88 T01110100,0000T0T—————o01111—HOIII]t 1f1Tgr m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 6.80 7.00 7.20 7.40

26133.D NP112601.M Mon Dec 03 10:07:11 2001 Page 1

NYC-WTC_000031035