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GCMS analysis report, Sample AD26164, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD26164 for unknown compounds conducted on December 3, 2001.

NYC-WTC_000031076–000031087

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26165.D Vial: 62 Acq On : 1 Dec 2001 2:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 d-Arabinose, cyclic 1,2-ethane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.02 0.73 ug/1 142249 1,4-Dichlorobenzene-d4 11.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 d-Arabinose, cyclic 1,2-ethanediyl 394 C15H2208S2 040733-16-2 64 2 Benzene, thiobis [chloro- 254 C12H8C12S 029349-72-2 25 3 2-Propanone ,/1-methoxy- 88 C4H802 005878-19-3 9 4 Ethyl Acetate 88 C4H802 000141-78-6 9 Abundance Scan 215 (7.015 min): 26165. D (-) m/z 42.95 100.00% 43

5000 61 II T T TIT TT i j it: TIT * TT[ * * 6.60 6.80 7.00 7.20 7.40 miz-> —4 "i ■■■*i 88 207 ' t i r» : | i i : i j : » i » | ! ti» y J i : i j < : i i । 1 i I i IT TIT TT • • ] TT I' I | I J I J | ri l l l l > J | I 20 40 60 03 100 120 140 160 180 200 220 240 260 280 300 320 m/z 44.9,5 91.29% Abundance #53382: d-Arabinose, cyclic 1,2-ethanediyl mercaptal, tetra 45 105

5000 i ■ ■ ■ • i ■ ' • • i • ‘ । 1 i ' 113 1uk 61 6.60 6.80 7.00 7.20 7.40 m/z 43.9.0 31.31% a . 85 _ w. 4 . J. jr _h t . ’ 1 ’111’11111717TTTI’T’’’TTA1’’TT 177 172 189 .... ...... mfz~> 20 40 00 80 100 120 140 160 180 200 220 240 260 280 300 320"" Abundance #34633: Benzene, thiobis[chloro- 45 75 6.60 6.80 7.00 7.20 7.40 5000 108 m/z 61.0,5 30.44%

1’________________________________________ 1’’271101101ITT ’11’11011101111001371 imp ‘ ‘" I ’' “ I' nlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #62920: 2-Propanone, 1-methoxy- 45 I Tff TI TT TB TIT ) II ! I | I 1 6.60 6.80 7.00 7.20 7.40 m/z 72.95 29.23% 5000 29

miz—> 14.1 n,| n irirrnju ‘‘I 88 20 40 60 80 100 120 140 160 180 200 220 24G 260 280 300 320 j TTTTTUOO]T 6.60 , RR +44 11T 6.80 7.00 7.20 7.40

26165.D NP112601.M Mon Dec 03 12:21:10 2001 Page 1

NYC-WTC_000031084

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NYC-WTC_000031084Source: NYC Law Department, mirrored locally

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