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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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Scanned page image, NYC-WTC_000031143
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OCR status: ok · source: pdftotext

NYC 9111 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\26205.D Vial: 68 Acq On : 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cyclopentasiloxane, decamethyl Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 14.34 2.56 ug/l 972039 Naphthalene-d8 15.31

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Cyclapentasilo ne, decamethyl- 370 C10H3005Si5 000541-02-6 59 2 Noradrenalin , tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 3 Benzoic ac' , 2,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 37 4 N-(Trifle oacet 1)-N,O,O',O''-tetr 553 C22H42F3NO4Si4 000000-00-0 32 bundance Scan 1012 (14.338 min): 26205.D (-) I m z 73.00 100.00 j

5000 267 355

45 108 133154 193 223 2 2g3 323 ii i p z 266. 43. > 40 60 80 100120140160180200220240260280300320340361 dance #51266: Cyclopentasiloxane, decamethyl-

355 267 5000 z 355. 207 323 > 40 60 80 100120140160180200220240260280300320340361 idance #57357: Noradrenaline, tetra-TMS

m/z .356.U5 1..3.-1U1 5000 102 355

`5 147 > 40 60 80 1001201401601802002202402602803003203403 ►dance #73975: Benzoic acid, 2,4-bis[(trimethyisilyl)oxv]-, trin' 14.00 14.20 14.40 14.60 Z 267.

5000 355 45 133 193 223 281

•> 40 60 80 10012014016018020022024026028030032034036

26205.D NP112601.M The Dec 04 15:58:40 2001 Page 6

NYC-WTC 000031143

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NYC-WTC_000031143Source: NYC Law Department, mirrored locally

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