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GCMS blank analysis results for sample AE10812, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing non-detect levels for 15 volatile organic compounds in a GCMS method blank processed on May 17-21, 2002.

NYC-WTC_000025499–000025507

Folder label: “GCMS X 5/17/02 A 5/16/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020521\0517LB2.D Vial: 4 Acq On : 21 May 2002 11:22 am Operator: Nefliu Sample : 05/17 lab blk ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.26 ug/1 24171 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 45 2 Pentacyclo[7. 3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 38 3 Boroxin, dimethylphenyl- 188 C8H11B303 1000162-59-8 35 4 Phenannhrene-dlO 188 C14D10 001517-22-2 25 Abundance Scan 4915 (31.958 min): 0517LB2.D (-4908) (-) m/z 188.10 100.00% 1t8

94 5000 158 44 84 66 119 148

mfe-> 0- L 1 .......ij..... II,... i ■ " ' i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 " i"1 31.60 31.80 32.00 32.20 m/z .94.20 66.09%

Abundance #79826: Anthracene-d10- 188

5000 31.60 31.80 32.00 32.20 m/z 187.20 43.83%

/z-> Abundance 17 42 52 1166 30 80 94 146—441791794 108118 132 0 1111" I" " I" " 11"11111 11 ■ I" 111"11 [ TT—ut 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 160

#79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )tetradeca... u its

31.60 31.80 32.00 32.20 5000 79 91 m/z 158.10 32.66% 55 67 131 105 117 Opus............. will U 1145/158.173.. 11„. . -44——1111111011111001100111—0000111—2 niz-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #79824: Boroxin, dimethylphenyl- 188 + 31.60 31.80 32.00 32.20 m/z 160.10 28.43% 173 5000 104 131 69 o= 146 ......................................................

n/z—> 0 26,32,.51.69.1,78,17 -Hm TT 1111159 . | 117 111111rl'11’0 1111 1 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 31.80 32.00 32.20

0517LB2.D SCAN020521.M Tue May 28 11:28:50 2002 Page 5

NYC-WTC_000025506

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NYC-WTC_000025506Source: NYC Law Department, mirrored locally

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